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Synthesis of Ethyl 2-(tosyloxy)acetate(3). Dissolve ethyl glycolate(1) and p-toluenesulfonyl chloride(2) in tetrahydrofuran (THF) in a 1:1 equivalent, add triethylamine dropwise at 0 °C. When TLC ...

2-Tosyloxy-1,3-propanediol (TPD), a potential precursor for 1,3-propanediol (1,3-PD) production, is produced by the tosylation of glycerol with the help of protecting group techniques. In this work, ...

Proteolysis-targeting chimeras (PROTACs) have received tremendous attention as a new and exciting class of therapeutic agents that promise to significantly impact drug discovery. These bifunctional ...

ABSTRACT: A mild, general, convenient, and efficient one-pot synthesis of 4-arylpyridines (4) is described using conventional heating, ultrasound and microwave irradiation. Aryl aldehydes (2) were ...

ABSTRACT: Ketones smoothly reacted with NBS in the presence of a catalytic amount of ptoluenesulfonic acid to give α-bromoketones in good yields in typical ionic liquids, such as [bmim]PF6 and ...